Thursday 10 May 2018

SOP OF Determination Of NOISE


Principle:       
To describe the general test method for measurement of noise.


Scope:              
This work instruction is applicable for measurement of noise at various locations.


Procedure:                                                
INSTRUMENT: Environmental noise pollution monitor
                        

Test method:                                                

Switch on the instrument by DC switch.                                 
    
Check the instrument for 94 dB(A) for its normal operation before taking for measurement

Place the monitor in such a way that the sensor of the monitor is facing the noise.

Keep the setting of four switches as under                           
                   ON / OFF        -  ON (DC) 
                   Range                   50 - 100
                   Selector switch -  A
                   Hold max          -  F

Equipment directly indicates the noise level.                        

Record the observation.


SOP Of Temperature


Scope:
Prescribes method for the measurement of temperature of water & waste water.


Principle:
            Temperature measurements may be made with any mercury-in-glass thermometer, provided it is checked occasionally against a precision thermometer certified by a competent agency. Depth temperature may be obtained with a protected reversing thermometer or a thermister. Measurements of temperature are, usually, more conveniently done using thermistors.

Procedure:

            Make measurement with the thermometer immersed directly in the water body, after a period of time sufficient to permit constant reading. If the measurement of water temperature cannot be carried out directly, carry it out in a sampling bottle. The bottle should have a volume of at least one litre. Adjust its temperature to that of the sample water before the measurement. Do not expose it to heat or direct solar radiation. Measure temperature of tap water in a bottle through the water flows until a constant reading is obtained. Make measurement of the temperature of a water body at a particular depth with the thermometer or thermistor immersed directly in the water body. After sufficient time has elapsed to allow the thermometer or thermistor to come to the exact temperature of the water, take a reading. In the case of the thermistor make a direct measurement of its resistance & obtain the temperature of the water body from the calibration curve supplied with the thermistor.
            In the case of reversing thermometer, obtain the reading by dropping a messenger weight along the wire to which is attached the reversing thermometer in a reversing frame on a water sampling bottle. This weight normally drops at a speed of about 150 meters per minute except when the wire is extremely inclined to the vertical. After sufficient time has passed for the messenger weight to trip the thermometer, haul up the wire & keep the water bottle with the thermometer carefully in a vertical position away from direct sunlight in order to prevent accidental reversing before reading the temperature to be measured. Allow about 10 to 15 minutes for the thermometers to reach the air temperature, after they are brought up from the water. At this stage the auxiliary thermometer records the atmospheric temperature & the main thermometer, the approximate temperature of the water body.

Calculations:  Calculate the exact temperature of the water body, in the case of the reversing thermometer, from the following formula:
                                        Tw = T΄+C+l
                              &        C = (T΄-Vo) (T΄-T1) / K – 100

Where
            Tw = The corrected value, that is, the true value of the water temperature, °C
            T’ – the reading of the main thermometer , °C
            I - the index correction given on a calibration sheet supplied with the thermometer            
            C- correction for thermal expansion
            V0 – volume of mercury below 0°C mark given on the calibration graph
            K – reciprocal thermal expansion coefficient given on the calibration graph, and
           T1 – temperature reading of the auxiliary thermometer , °C

If an unprotected reversing thermometer is used along with the protected thermometer the corrected temperature Tu can be similarly obtained. The actual depth of reversal of the thermometers can be obtained using the following equation

                      Z      =           Tu – T w
                                           Pm – Q  
            Where,

                        Z  = depth in metres
                        Tu = corrected reading of the protected thermometer, °C
                        Tw = corrected reading of the protected thermometer , °C
                        Pm = mean density of the water column
                        Q = pressure coefficient of the unprotected thermometer given on the  
       calibration graph

Report:
Report the temperature of water to the nearest 0.01 , 0.1 or 0.5°C , depending on the accuracy required and the thermometer used.
    

SOP OF ESTIMATION OF ODOUR

PREPARATION OF APPARATUS:

Thoroughly clean the required number of wide-mouth glass Stoppered bottles of about one litre capacity. Rinse them with hydrochloric acid and render them completely odourless by repeated washing with odour free distilled water through a column of granulated activated carbon.

PROCEDURE:

As soon as possible after collection of sample, fill a bottle, half full of sample, insert the stopper, shake vigorously for 2 to 3 seconds and then clean quickly observe the odour. The sample taken for observation of odour shall be at room temperature.

REPORT:

Report the true odour of the sample at the mouth of the bottle as rotten egg, burnt sugar, soapy, fishy, septic, aromatic, chlorinous, alcoholic odour or any other specific odour. In case it is not possible to specify the exact nature of odour, report as agreeable or disagreeable.


ODOUR CLASSIFIED BY CHEMICAL TYPES


ODOUR CHARACTERISTICS

SWEETNESS
(1)
PUNGENCY
(2)
SMOKINESS
(3)
ROTTENNESS
(4)
ODOUR CLASS (5)
100
50
0 to 50
50
Estery
100
50 to 100
0 to 100
50
Alcoholic
50
50
0 to 50
50
Carbonyl
50
100
0 to 50
50
Acidic
100
50 to 100
50 to 100
0 to 100
Halide
50
50
100
100
Sulphury
100
50
50
100
Unsaturated
100
50
0 to 50
100
Basic






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